Solid-state NMR
PFIS-2020 / PQUI-335
Prof. Jair C. C. Freitas
Classroom presentations:
- Lecture 1: Introduction to NMR – Nuclear properties.
- Lecture 2: Introduction to NMR – Spin precession and nuclear paramagnetism.
- Lecture 3: Introduction to NMR – Rotating frame, RF pulses and the NMR signal.
- Lecture 4: Introduction to NMR – FIDs, Fourier transform and NMR spectra.
- Lecture 5: NMR relaxation – General principles, transverse relaxation and magnetic field inhomogeneity.
- Lecture 6: NMR relaxation – Spin echoes, CPMG pulse sequence.
- Lecture 7: NMR relaxation – Longitudinal relaxation.
- Lecture 8: NMR relxattion – Relaxometry and applications.
- Lecture 9: NMR relaxation – Fluctuating fields.
- Lecture 10: Quantum description of NMR experiments.
- Lecture 11: NMR instrumentation – spectromenter, transmitter, duplexer.
- Lecture 12: NMR instrumentation – RF probes, signal reception, processing of FIDs and spectra.
- Lecture 13: Nuclear spin interactions – Nuclear spin Hamiltonian, chemical shift.
- Lecture 14: Nuclear spin interactions – Direct dipolar coupling, J-coupling.
- Lecture 15: Nuclear spin interactions – Hyperfine interactions, magnetic materials.
- Lecture 16: Nuclear spin interactions – Electric quadrupole coupling.
- Lecture 17: High-resolution solid-state NMR methods – Magic angle spinning (MAS).
- Lecture 18: High-resolution solid-state NMR methods – Decoupling.
- Lecture 19: High-resolution solid-state NMR methods – Cross polarization (CP).
- Lecture 20: High-resolution solid-state NMR methods – MAS and quadrupole effects.
- Lecture 21: Advanced solid-state NMR methods – spectral edition and 2D methods.