Solid-state NMR

PFIS-2020 / PQUI-335

Prof. Jair C. C. Freitas

Suggested texts:

“Os núcleos atômicos e a RMN”, J. C. C. Freitas, T. J. Bonagamba. In: J. D. Figueroa Villar (editor), Fundamentos e Aplicações da Ressonância Magnética Nuclear, n. 1, AUREMN, 1999.

“New Zealand developments in Earth’s field NMR”, P. T. Callaghan, A. Coy, R. Dykstra, C. D. Eccles, M. E. Halse, M. W. Hunter, O. R. Mercier, J. N. Robionson. Appl. Magn. Reson. 2007;32:63-74.

“Nuclear magnetic resonance for the people”, P. J. Grandinetti.

“NMR and nomenclature. Nuclear spin properties and conventions for chemical shifts (IUPAC Recommendations 2001)”, R. K. Harris, E. D. Becker, S. M. Cabral de Menezes, R. Goodfelow, P. Granger. Pure Appl. Chem. 2001;73:1795-1818.

“Further conventions for NMR shielding and chemical shifts (IUPAC recommendations 2008)”, R. K. Harris, E. D. Becker, S. M. Cabral de Menezes, P. Granger, R. E. Hoffman, K. W. Zilm. Pure Appl. Chem. 2008;80:59-84.

“NMR signal reception: virtual photons and coherent spontaneous emission”, D. I. Hoult, B. Bhakar. Concepts Magn. Reson. 1997;9:277-297.

“Simple laboratory experiments to observe the manifestations of the sinc function”, D. D. Traficante, M. M McGregor. Concepts Magn. Reson. 2002;14:308-325.

“The effects of finite rectangular pulses in NMR: phase and intensity distortions for a spin-1/2”, R. M. Gregory, A. D. Bain. Concepts Magn. Reson. 2009;34A:305-314.

“Single- and multiple-frequency-shifted laminar pulses”, S. L. Patt. J. Magn. Reson. 1992;96:94-102.

“Spin echoes”, E. L. Hahn. Phys. Rev. 1950;80:580-594.

“Effects of diffusion on free precession in nuclear magnetic resonance experiments”, H. Y. Carr, E. M. Purcell. Phys. Rev. 1954;94:630-638.

“Modified spin–echo method for measuring nuclear relaxation times.” S. Meiboom, D. Gill. Rev. Sci. Instrm. 1958;29:688–691.

“Proton-enhanced NMR of dilute spins in solids”, A. Pines, M. G. Gibby, J. S. Waugh. J. Chem. Phys. 1973;59:569.

“Practical aspects of modern routine solid-state nuclear magnetic resonance spectroscopy: one-dimensional experiments”, D. L. Bryce, G. M. Bernard, M. Gee, M. D. Lumsden, K. Eichele, R. E. Wasylishen, Can. J. Anal. Sci. Spectr. 2001;46:46.

“NMR in rotating solids”, M. M. Maricq, J. S. Waugh. J. Chem. Phys. 1979;70:3300-3316.

“Interações hiperfinas”, I. S. Oliveira, A. P. Guimarães, Revista Brasileira de Ensino de Física 2000;22:353-359.

“Aplicações da ressonância magnética nuclear ao estudo de materiais magnéticos”, A. P. Guimarães, Revista Brasileira de Ensino de Física 2000;22:360-362.

“Recent advances in experimental solid state NMR methodology for half-integer quadrupolar nuclei”, M. E. Smith, E. R. H. van Eck, Prog. Nucl. Magn. Reson. Spec. 1999;34:159-201.

“Nuclear resonance in hydrated crystals: fine structure of proton line”, G. E. Pake, J. Chem. Phys. 1948;16:327-336.

“Aplicações da ressonância magnética nuclear ao estudo de materiais magnéticos”, A. P. Guimarães. Revista Brasileira de Ensino de Física 2000;22:360-362.